I believe everyone knows the importance of the neck. It is the fixation device for various organs. With the increase of work pressure and unhealthy lifestyle, many people suffer from neck diseases. Many people think that it is an unimportant disease that will not cause death, but this is actually wrong. Neck Pain Medicine Wine is a good remedy for treating neck diseases. Although many people have used it, they do not understand its identification method and effectiveness. Let me introduce to you its identification method and effectiveness. Identification method: (1) Take 100 ml of the product and place it in an evaporating dish. Heat it on a water bath until there is no alcohol smell. Cool it and add 50 ml of ether to extract it. Separate the ether layer and evaporate it to dryness. Add 1 ml of chloroform to the residue to dissolve it and use it as the test solution. Take another rhein reference substance and add chloroform to make a solution containing 0.4 mg per 1 ml as the reference substance solution. According to the thin layer chromatography test, 6μl of the test solution and 3μl of the reference solution were respectively spotted on the same silica gel G thin layer plate, and the upper layer solution of petroleum ether (30-60℃)-ethyl formate-formic acid (15:5:1) was used as the developing agent. The plate was developed, taken out, dried, and examined under ultraviolet light (365nm). In the chromatogram of the test sample, a fluorescent spot of the same color appears at the corresponding position in the chromatogram of the reference sample; after being fumigated with ammonia gas and examined under sunlight, the spot turns red. (2) Take 1 g of Angelica sinensis as a control medicinal material, add 10 ml of chloroform, and treat with ultrasound for 15 minutes. Filter and evaporate the filtrate on a water bath to dryness. Add 1 ml of chloroform to the residue to dissolve it and use it as the control medicinal material solution. According to the thin layer chromatography test, take 3 μl of the above-mentioned reference solution and the test solution under identification (1), respectively, and spot them on the same silica gel G thin layer plate, use n-hexane-ethyl acetate (9:1) as the developing solvent, develop, take out, dry, and examine under ultraviolet light (365nm). In the chromatogram of the test sample, fluorescent spots of the same color appear at the corresponding positions in the chromatogram of the control medicinal material. (3) Take the aqueous layer from identification (1) and extract twice with 40 ml of water-saturated n-butanol each time. Combine the n-butanol solutions and wash with 50 ml of ammonia test solution. Take the n-butanol solution and evaporate it to dryness on a water bath. Add 1 ml of methanol to the residue to dissolve it and use it as the test solution. Take another reference substance of paeoniflorin and add methanol to prepare a solution containing 1 mg per 1 ml as the reference substance solution. According to the thin layer chromatography test, 3 μl of each of the above two solutions were taken and spotted on the same silica gel G thin layer plate, and benzene-methanol-ethyl acetate-ammonia water (10:4:2:0.5) was used as the developing solvent. After development, the plate was taken out, dried, sprayed with anisaldehyde-glacial acetic acid-sulfuric acid (0.1:10:0.2) solution, and dried at 105°C for about 5 minutes. In the test sample chromatogram, a spot of the same color appears at the corresponding position in the reference sample chromatogram. effect: Neck pain remedy wine has the functions of nourishing the liver and kidneys, activating blood circulation and relieving pain. Used for pain caused by various cervical spondylosis. I believe that through the above content everyone has a more comprehensive understanding of the identification method and efficacy of Neck Pain Medicinal Wine. I hope these methods can help protect the neck. We can better improve our bodies to achieve the goal of protecting the neck, balancing nutrition and strengthening the body! Make your life more harmonious and beautiful while not harming your body. Although medicinal wine is good, don't drink too much. |
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